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- W2363916284 abstract "OBJECTIVE:To establish a high performenc capillary zone electrophoresis method for the determination of the water-soluble active ingredients in different parts of the Salvia miltiorrhiza.METHODS:Capillary electrophoresis was conducted using uncoated capillary column(75 μm×50.2 cm,effective length=40 cm)with 5 mmol·L-1 phosphate-borax(ph7.4)as running buffer by pressure injection(0.5 psi/4 s)and constant voltage separation(20 kV)with a detection length of 210 nm and a column temperature of 25 ℃.RESULTS:A complete baseline separation of PAH,DSS and PA was achieved within 8 min under the optimized conditions.The good linear range was from 2.5 μg·mL-1 to 200.0 μg·mL-1 for all the three ingredients.The average recoveries of the 3 ingredients were 100.04%,99.99%,and 100.01%,respectively,with RSD at 1.75%,1.73%,and 1.74%,respectively.CONCLUSION:The method is satisfactory in precision,recovery and linearity,and it can be used to determine three water-soluble active ingredients in different parts of the Salvia miltiorrhiza." @default.
- W2363916284 created "2016-06-24" @default.
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- W2363916284 date "2008-01-01" @default.
- W2363916284 modified "2023-09-22" @default.
- W2363916284 title "Determination of Water-soluble Active Principles in Different Parts of Salvia miltiorrhiza by Capillary Zone Electrophoresis" @default.
- W2363916284 hasPublicationYear "2008" @default.
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