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- W2364117791 abstract "The reaction system (NH 4) 3VS 4/Et 4NBr/CuBr/PPh 3 in CH 2Cl 2 for self-assembling of [VS 4-Cu n ] ( n from 3 to 6) clusters was simulated in NMR tube. After the relationship between the 51V NMR chemical shifts and the number of copper atoms in this family cluster was established theoretically and experimentally, 51V NMR was used as a pseudo in situ and real-time method to monitor and identify possible products during the reaction process. The reaction conditions and mechanism about the formation of [VS 4-Cu n ] clusters were investigated by changing the molar ratios of the reactants. The results showed that the concentration of PPh 3 has obvious influence on the 51V chemical shift, and their mechanism is discussed in detail." @default.
- W2364117791 created "2016-06-24" @default.
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- W2364117791 date "2001-01-01" @default.
- W2364117791 modified "2023-09-25" @default.
- W2364117791 title "~(51)V NMR STUDIES ON THE REACTION OF [VS_4-Cu_n] (n=3-6) CLUSTERS" @default.
- W2364117791 hasPublicationYear "2001" @default.
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