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- W2364263752 abstract "Graphite oxide( GO) was prepared with a mixture of concentrated H2SO4 / H3PO4 to replace NaNO3 / KClO3 which are easy to produce poison,by KMnO4 as oxidizing agent and flake graphite as carbon source. To obtain fully oxidized GO,the effects of the quantity of graphite,quantity of KMnO4,reaction time, and temperature on the degree of oxidization of GO were evaluated by the orthogonal array design( OAD). And the optimum preparing conditions of GO obtained by the improved preparation were determined by range analysis. Graphite oxide structure obtained at the optimal parameters by the improved method was characterized by X-ray diffraction patterns( XRD),ultraviolet and visible spectroscopy( UV-Vis),and Raman spectrum,and was compared with GO produced by the Hummers method. The results indicate that the GO obtained by the improved synthesis method has fewer defects in the basal plane than the Hummers method." @default.
- W2364263752 created "2016-06-24" @default.
- W2364263752 creator A5080650589 @default.
- W2364263752 date "2013-01-01" @default.
- W2364263752 modified "2023-09-25" @default.
- W2364263752 title "Orthogonal Design of Graphite Oxide Prepared by Improved Technology" @default.
- W2364263752 hasPublicationYear "2013" @default.
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