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- W2364278513 abstract "A method of GC for the determination of 1-deoxynojirimycin(DNJ) in mulberry leaves was proposed.DNJ in the extract of mulberry leaves was derivatized with hexamethyldisilazane and trimethylchlorosilane at 60 C for 0.5 h.The derivatized product was separated on TRB5 column(30 m×250μm,0.50μm),determined by FID,and detected qualitatively by GC-MS.Linear relationship between values of peak area and mass concentration of DNJ was kept in the range of 0.01-0.10 g ? L~1,with detection limit(3S/N) of 0.06 mg ? L~1.The proposed method was applied to the analysis of extract of mulberry leaves,giving values of RSD(n = 6) of1.9%,and recovery in the range of 101%-103%." @default.
- W2364278513 created "2016-06-24" @default.
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- W2364278513 date "2013-01-01" @default.
- W2364278513 modified "2023-09-25" @default.
- W2364278513 title "GC Determination of 1-Deoxynojirimycin in Mulberry Leaves Derivatized with Silanes" @default.
- W2364278513 hasPublicationYear "2013" @default.
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