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- W2364280136 abstract "The Polycaprolactone(PCL) cast film was made using purified PCL,the purified CHCl3 acted as solvent.The specimen was investigated by using modulated thermogravimetry analysis,the structure of low molecular compounds were determined by NMR and FTIR.It can be found from results of modulated TGA that the PCL pyrolysis had two steps,the decomposition temperature and the weight loss rate in the first step were 205~295℃ and 7.0% respectively,while in the second were 311~374℃ and 88%.At the same time the Ea,Z and ln[rate ratio] be got,in the first step the results were respectively 80kJ/mol,5min-1 and 0.3,as in the second were 146kJ/mol,11min-1 and 0.47.And the result of the NMR and FTIR suggested that during the pyrolysis process,not only be get macromoleclar PCL,but also the furan,cyclopropanes displaced unsaturation carboxylic acid were produced." @default.
- W2364280136 created "2016-06-24" @default.
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- W2364280136 date "2011-01-01" @default.
- W2364280136 modified "2023-09-27" @default.
- W2364280136 title "Thermal Degradation Mechanism and Pyrolysis of thePolycaprolactone" @default.
- W2364280136 hasPublicationYear "2011" @default.
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