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- W2364316663 abstract "Epichlorokydrin was prepared with glycerol by the catalysis of the prepared catalyst,which was a polymer with ketone radical/sulfone radical in backbone chain and carboxy.The catalyst was stable in the reaction mixture and could be reused.The reactivity and selectivity of the catalyst were high,of which the selectivity was more than 94% to 1,3-dichloro-2-propanol and no 1,2,3-trichloropropane.The yield of dichloropropanol could be achieved to 98%(99.5% purity) when the reaction temperature and the dosage of the catalyst were 110℃ and 5%(based on the weight of glycerol).By the reaction of dichloropropanol with sodium hydroxide,the yield of epichlorophydrin could achieve 91%(96% purity) while the concentration of caustic soda,the mol ratio of caustic soda to dichloropropanol,the reaction temperature and the reaction time were 25%,1.02/1,55℃ and 1 h,respectively.The purity of epichlorophydrin could be 99.8% by fractional distillation." @default.
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- W2364316663 date "2008-01-01" @default.
- W2364316663 modified "2023-09-24" @default.
- W2364316663 title "Study on a new catalyst and technology for preparation of epichlorokydrin from glycerol" @default.
- W2364316663 hasPublicationYear "2008" @default.
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