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- W2364402062 abstract "2-(p-Methoxyphenyl)-1H-benzo[d]imidazole was efficiently synthesized from p-methoxybenzaldehyde and o-phenylenediamine under microwave irradiation by air oxidation method without any catalyst for the first time.The effects of microwave irradiation power,microwave irradiation time,molar ratio,and solvent amount on the yield of object compound were investigated.The results showed that the optimum reaction conditions are as follows:microwave irradiation power 280 W,radiation time 5.0 min,n(p-methoxybenzaldehyde)∶n(o-phenylenediamine) = 1.1∶1.0,amount of ethanol 6.0 mL,the highest yield of the title compound was up to 88.7%." @default.
- W2364402062 created "2016-06-24" @default.
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- W2364402062 date "2011-01-01" @default.
- W2364402062 modified "2023-09-22" @default.
- W2364402062 title "Synthesis of 2-(p-methoxyphenyl)-1H-benzo[d]imidazole under microwave irradiation by air oxidation method" @default.
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