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- W2364432859 abstract "Residual amounts of ten carbamate pesticides in vegetables and fruits were determined by LC-MS/ MS.Samples of vegetables or fruits were extracted with acetonitrile.Sample solution in CH_3OH-CH_2Cl_2(1+99) was purified by SPE and the eluate,after evaporation to near dryness by N_2-blowing and dissolution in 1 mL of acetonitrile,was used for LC-MS/MS determination,with C_(18) chromatographic column and gradient elution using acetonitrile and methanol-water mixed solution as mobile phase.Detection limits(3S/N) for the 10 pesticides found were 1μg·kg~(-1).Recovery of the method was tested at 3 concentration levels of 1,10,100μg·kg~(-1) for each of the 10 pesticides,values of recovery found for savoy were ranged from 78.5%to 105.0%and for orange were ranged from 80.3%to 106.0%,with values of RSD's(n=6) in the ranges of 4.6%-19.8%and 3.5%-17.7% respectively." @default.
- W2364432859 created "2016-06-24" @default.
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- W2364432859 date "2009-01-01" @default.
- W2364432859 modified "2023-09-23" @default.
- W2364432859 title "LC-MS/MS Determination of Residual Amounts of Carbamate Pesticides in Vegetables and Fruits" @default.
- W2364432859 hasPublicationYear "2009" @default.
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