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- W2364474294 abstract "A facile one-pot procedure for the preparation of diethyl N-carbobenzyoxy-or N-acetyl-α-aminoalbylphosphonates from the condensation of relevant aldehydes,amides andphosphorus trichloride was described.A tentative reaction mechanism was proposed anddiscussed.The crystal and molecular structure of dietheyl N-acetyl-α-amino-γ-methyl bu- tylphosphonate(g)and by product N-[α-isopropyl-5-methylhexadienyl-(1,3)]-acetamide(h)were determined by X-ray diffraction.The crystal of(g)belongs to a P(?) space groupwith lattice parameters:α=8.688(4),b=8.990(3),c=10.309(2);α=87.89(2),β=83.63(2),γ=88.27(3)and the crystal of(h)belongs to Pna 2_1 space group,the latlice parame-ters are α= 9.326(4),b=14.276(3),c=9.843(2)." @default.
- W2364474294 created "2016-06-24" @default.
- W2364474294 creator A5002596518 @default.
- W2364474294 date "1989-01-01" @default.
- W2364474294 modified "2023-10-17" @default.
- W2364474294 title "Synthesis of Diethyl N-Acyl-α-aminoalkylphosphonates and Determination of their Molecular Structures" @default.
- W2364474294 hasPublicationYear "1989" @default.
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