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- W2364485983 abstract "Fire retardant additive 2,4, 6-tri-(2, 4, 6-tribromophenyloxyl)-1,3, 5-triazine was synthesized with tetramethylammonium chloride as catalyst by tribromophenol and cyanuric chloride in toluene. The hydrochloride was eliminated and no water was released in the reaction process and therefore the vice reaction (hydrolysis) was avoided. The yield reached above 99 % . The reaction would finish in 8 h with 2 % catalyst and the reaction time decrease 4h than that with 1 % catalyst. Comparing with the products prepared under water-containing condition, there were no obvious hydrolysis vice products. Comparing with the system prepared in ethyl acetate,the products didn't contain vice products which reactioned with ethyl acetate." @default.
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- W2364485983 date "2009-01-01" @default.
- W2364485983 modified "2023-09-26" @default.
- W2364485983 title "Synthesis of Tri-(tribromobenoxyl) -triazine with Eliminating Hydrochloride in Solvent" @default.
- W2364485983 hasPublicationYear "2009" @default.
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