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- W2364490169 abstract "OBJECTIVE To optimize the purification process of total flavones from Bushen Recipe with macroporous resin DM301. METHODS Based on orthogonal design,the contents of total flavones and the contents of stilbeneglycoside,icarrin and naringin worked as indexes,the factors such as adsorption capacity,the column diameter-height ratio,eluant volume and elution velocity were investigated,as well as the changes of the portions of the indicial components before and after purification. RESULTS The optimum elution parameters were as follows: the column diameter-height ratio was 1∶10,the eluant volume of 70% alcohol was 4 BV and elution velocity was 2.3 BV·h-1,respectively.The purity of the total flavones extract was more than 50%,the reservation rate was 76.30%,and the yield was 2.25%(calculating with crude material).The portions of three indicial components before and after purification were nearly same. CONCLUSION The purification process can significantly improve the purity degree and decrease the yield of extract,and thus the administrated amount of the drug was decreased." @default.
- W2364490169 created "2016-06-24" @default.
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- W2364490169 date "2011-01-01" @default.
- W2364490169 modified "2023-09-22" @default.
- W2364490169 title "Optimum research on purification process of total flavones from Bushen Recipe with macroporous resin DM301" @default.
- W2364490169 hasPublicationYear "2011" @default.
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