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- W2364640002 abstract "The synthetic method of bis-(o-trifluoromethylphenyl)dithiophosphinic acid has been improved during the synthetic research of various dithiophosphinic acids.The optimized synthesis has been realized with PCl3 and(o-F3CC6H4)MgBr as starting materials and via a continuous three-step method including Grignard reaction,sulfuration and substitution reaction.The FTIR spectrum of product shows the presence of substituted aromatic ring,C-F bond,P-S single bond and P=S double bond.The interpretation result of 31P NMR,1H NMR and 13C NMR of the product,as well as MS,is completely in line with the structure of the targeted compound bis-(o-trifluoromethylphenyl)dithiophosphinic acid." @default.
- W2364640002 created "2016-06-24" @default.
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- W2364640002 date "2010-01-01" @default.
- W2364640002 modified "2023-09-26" @default.
- W2364640002 title "Synthesis of Bis-(o-Trifluoromethylphenyl) Dithiophosphinic Acid" @default.
- W2364640002 hasPublicationYear "2010" @default.
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