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- W2364656244 abstract "Objective:To establish a quality control method for Jianweiling granules.Methods:The two main ingre- dient of Radix Astragali and Radix Angelicae Sinensis were identified by silical gel G thin layer chromatography and the paeoniflorin was determined by RP-HPLC with a Ultimate~(TM)XB-C_(18)(5μm,4.6 mm×250 mm)column.The mobile phase was methanol-aeetonitrile-potassium dihydrogen phosphate(22:15:63).The flow rate was 0.6 mL ·min~(-1).The detection wavelength was 230 nm.Results:The calibration curve was linear in the range of 9.64- 96.4μg·mL~(-1)for paeoniflorin with r=1.000.Within-day RSD and between-day RSD were 1.0% and 1.8% (n=3).The average recoveries of high,middle and low concentrations of sample were 101.2%,100.8%,101.1% with RSD=1.3%,1.0% ,0.58%(n=3).Conclusions:The methods are simple,reproducible,accurate and relia- ble,which is used for the quality control of the Jianweiling granules." @default.
- W2364656244 created "2016-06-24" @default.
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- W2364656244 date "2007-01-01" @default.
- W2364656244 modified "2023-09-23" @default.
- W2364656244 title "Studies on the quality control method of Jianweiling granules" @default.
- W2364656244 hasPublicationYear "2007" @default.
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