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- W2364706786 abstract "Objective:To establish a GC method for simultaneous determination of 4 compounds(α-pinene,β-pi- nene,limonene,and bornyl acetate)in volatile fractions of Schisandra chinensis(Turcz.)Baill.Methods:The es- sential oil was extracted by steam distillation.GC method was applied for the determination of α-pinene,β-pi- nene,limonene,and bornyl acetate from the essential oil.Chromatographic conditions:Capillary column DB-17(30 m×0.25 mm×0.25μm)was used;The detector was FID;Inlet temperature was 230℃;The detector temperature was 250 ℃;Column temperature:50℃(2 min)130℃(5 min);Carrying gas was nitrogen(1.2 mL· min~(-1),split ratio was 10:1;Injection volume was 1μL.Results:The linear ranges for α-pinene,β-pinene,lim- onene and bornyl acetate were 0.02-0.21 mg·mL~(-1)(r=0.9998),0.006-0.10 mg·mL~(-1)(r=0.9993), 0.006-0.16 mg·mL~(-1)(r=0.9994)and 0.04-1.00 mg·mL~(-1)(r=0.9993),respectively;The average recov- eries(n=3)of α-pinene,β-pinene,limonene and bornyl acetate were 99.5%-101.6%,96.3%-101.9%, 98.6%-100.4%,96.1%-96.8%,respectively.Conclusion:This method is simple,quick and specific.It can be applied for the simultaneous determination of 4 compounds(α-pinene,β-pinene,limonene,and bornyl acetate) in volatile fractions of Schisandra chinensis(Turcz.)Baill." @default.
- W2364706786 created "2016-06-24" @default.
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- W2364706786 date "2008-01-01" @default.
- W2364706786 modified "2023-09-27" @default.
- W2364706786 title "GC simultaneous determination of α-pinene,β-pinene,limonene and bornyl acetate in volatile fractions of Schisandra chinensis(Turcz.) Baill." @default.
- W2364706786 hasPublicationYear "2008" @default.
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