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- W2365070007 abstract "The organic template P123(EO20PO70EO20) has been recovered from SBA-15 molecular sieves using solvent extraction with three different solvents.The effects of extraction solvent type,extraction temperature,extraction time and extraction solvent dose on the recovery ratio were studied.The results showed that under the optimal operating conditions with methanol as solvent,extraction temperature of 75 ℃,extraction time of 3.5h,and extraction solvent dose of 300 mL,the template P123 recovery ratio was 80.7%.The extracted SBA-15 was characterized by X-ray diffraction(XRD),thermogravimetric analysis(TGA),Fourier transform infrared spectroscopy(FT-IR) and N2 adsorption-desorption isotherms.The recovered SBA-15 had a more ordered framework and a higher surface area than samples from which the template had been removed by calcination,showing that template recovery by solvent extraction can avoid the structure shrinkage and silanol group removal caused by high temperature calcination.The recovered P123 was characterized by Fourier transform infrared spectroscopy(FT-IR) and gel permeation chromatography(GPC),and was identical to the reference P123 sample." @default.
- W2365070007 created "2016-06-24" @default.
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- W2365070007 date "2013-01-01" @default.
- W2365070007 modified "2023-09-25" @default.
- W2365070007 title "Recovery of the organic template from SBA-15 using solvent extraction" @default.
- W2365070007 hasPublicationYear "2013" @default.
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