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- W2365084576 abstract "Using 3-methyl amino-2-acid ethyl ester and p-benzoquinone as raw materials,in dichloroethane,zinc chloride catalyst,HPLC tracking detection synthesis Mecarbinate.Using orthogonal design,the optimal process parameters:reaction time 1~2 h,reaction temperature 55 ℃,molar ratio of n(p-benzoquinone)∶ n(3-methyl amino-2-acid ethyl ester)=1∶ 1.19,n(p-benzoquinone)∶ n(zinc chloride)=1∶0.32.Under the optimum conditions the yield of 85%,and the purity of more than 98%,to reached the purpose of optimization." @default.
- W2365084576 created "2016-06-24" @default.
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- W2365084576 date "2013-01-01" @default.
- W2365084576 modified "2023-09-26" @default.
- W2365084576 title "Research on Mecarbinate synthesis technology" @default.
- W2365084576 hasPublicationYear "2013" @default.
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