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- W2365399049 abstract "The determination of chloramphenicol in prawns was established by gas chromatography-mass spectrometry with negative chemical ionization (GC-NCI-MS). Chloramphenicol was extracted with ethyl acetate and particioned with -hexane to remove lipids. Cleanup was performed on a Diaion HP-20 column, and the recovered chloramphenicol was derived with BSTFA-TMCS and analyzed in selective ion monitoring (SIM) mode using m/z 466 as the characteristic ion. The linear range was very good from 5 to 500 #mu#g/L and relative coefficient was 0.9988. The detection limit was down to 0.037 #mu#g/kg. The average recovery rates were 71.33%-95.29% when 1-100 #mu#g/kg chloramphenicol standards were spiked into the zero shrimp sample, and the RSDs were 1.73%-7.45%. The chloramphenicol residues in the coltured Penaeus vannamei muscle obtained from karked was (0.154+-0.008) #mu#g/kg and no chloramphenicol residue was detected in the Palaemon carincauda muscle." @default.
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- W2365399049 date "2004-01-01" @default.
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- W2365399049 title "Determination of chloramphenicol residues in prawns by GC- NCI- MS" @default.
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