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- W2365475621 abstract "High performance liquid chromatography method was used to determin benzo(a)pyrene in preserved ham.By ultrasonic extraction and saponification,the working conditions of LC: separate column was Diamonsil C18(4.6mm×250mm,5μm),mobile phase was CH3CN-H2O,the excitation wavelength is 385nm,by fluorescence detector and detection wavelength is 405nm.The calibration curve was linear in the range of 0.050～1.0 μg/mL,Y=1.8×107x + 11012,R = 0.9992;added to 0.0035,0.0070 and 0.0105μg,their recovery rate was 83.08%,88.67% and 84.54%,respectively.The result show that the method has higher precision and accuracy in determination of benzo(a)pyrene.At the same time,the paper reported that content of benzo(a) pyrene preserved ham between 1.04～4.16μg/kg,which showed security of traditional preserved ham.had an impact on people's health." @default.
- W2365475621 created "2016-06-24" @default.
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- W2365475621 date "2008-01-01" @default.
- W2365475621 modified "2023-09-27" @default.
- W2365475621 title "Determination of benzo(a)pyrene in preserved ham by high performance liquid chromatography-fluorescence detector" @default.
- W2365475621 hasPublicationYear "2008" @default.
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