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- W2365634832 abstract "An efficient, sensitive, and low matrix interference method for the determination of chloramphenicol(CAP) and florfenicol(FF) in fishery products using gas chromatography-electron capture detector(GC-ECD) has been developed. Samples were treated by extraction with ethyl acetate and n-hexane purification. Further cleanup of the extracts was processed by a modified dispersive solid phase extraction procedure. Then, the purifi ed solutions were derivatized with slilyl reagents. The linearity of the method ranged from 1.5 to 100 μg/L for CAP, and from 6 to 400 μg/L for FF, with correlation coeffi cients ranging between 0.998 1 and 0.999 7. The limits of detection were 0.1–0.3 μg/kg. The recoveries of spiked CAP and FF with external calibration method at different concentration levels in different sample matrixes(crucian, blue crab, and Penaeus vannawei) were 82%–106%, 87%–111%, and 91%–98%, respectively, with relative standard deviations of 2.3%–4.9%, 2.4%–4.5%, and 1.4%–4.1%(n = 5), respectively. Thus it is concluded that this method can be successfully applied for the determination of choramphenicols(CAPs) in fishery products." @default.
- W2365634832 created "2016-06-24" @default.
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- W2365634832 date "2014-01-01" @default.
- W2365634832 modified "2023-09-24" @default.
- W2365634832 title "Determination of Chloramphenicol and Florfenicol in Fishery Products by Using Dispersive Solid Phase Extraction and Gas Chromatography" @default.
- W2365634832 hasPublicationYear "2014" @default.
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