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- W2365745575 abstract "Two synthetic methods of 1,2-Benzisothiazol-3(2H)-one-2-butyl-1,1-dioxide(Thiazone,a novel skin penetration enhancer),such as the phase transfer catalysis method and DMF(N,N-dimethyllformamide) solvent method,were studied.Attention was paid to improving the DMF solution method.The yield of Thiazone was reached over 88 % by using the improved DMF solvent method at reaction temperature 100 ℃ and feed mole ratio 1∶1∶10 of sodium saccharin,butyl bromide and DMF.DMF could be reused by reduced pressure distillation and its recovery rate was over 99 %.The product could be purified well though ethanol extraction and its purity was over 99%.The improved DMF solvent method has advantages in economy and industrialization." @default.
- W2365745575 created "2016-06-24" @default.
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- W2365745575 date "2009-01-01" @default.
- W2365745575 modified "2023-09-28" @default.
- W2365745575 title "Synthesis of novel penetration promoter Thiazone" @default.
- W2365745575 hasPublicationYear "2009" @default.
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