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- W2366069762 abstract "OBJECTIVE:To determine serum concentrations of phenbarbital(PB),phenytoin sodium(PHT),carbamazepine(CBZ)by micellar electrokinetic capillary chromatograph(MEKC).METHODS:The determination was performed on elastic quartz column(37 cm×50 μm)with barbital as internal standard.The buffer solution consisted of 10 mmol·L-1 phosphate sodium buffer-30 mmol·L-1 SDS sodium(micellar phase)-15% methanol at a constant voltage of 18 kV.The detection wavelength was set at 210 nm.RESULTS:The linear concentration ranges of PB and PHT were 2.5～80 μg·mL-1,with detective concentration of 0.1 μg·mL-1;the linear range and detective concentration of CBZ were 1～32 μg·mL-1 and 0.2 μg·mL-1,respectively.The average recoveries of the PB,PHT,and CBZ were 99.90%,99.91%,and 99.42%,respectively.CONCLUSION:The method is rapid,simple,accurate,sensitive and reproducible,and suitable for clinical monitoring of drug level and pharmaceutical study." @default.
- W2366069762 created "2016-06-24" @default.
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- W2366069762 date "2008-01-01" @default.
- W2366069762 modified "2023-09-23" @default.
- W2366069762 title "Determination of Serum Concentrations of Phenbarbital,Phenytoin Sodium and Carbamazepine by MEKC" @default.
- W2366069762 hasPublicationYear "2008" @default.
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