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- W2366127194 abstract "Agglomeration-freepowders with nanometer size were prepared by heterogeneous azeotropic distillation method.The surface chemical bonding between Zr(OH)4-Al(OH)3 gels and n-butanol,a dehydrator,was determined by FT-I.The powders had an average particle size 20nm in diameter and their green articles had one peak distribution of pores among the particles at 30nm,i.e.not existing as any hard agglomerates.Also the sintering temperature decreased 300℃ after the powders treated by the distillation,the bodies having 97.75% theoretical density and 0.2 grain size on sintering at 1300℃ for 4h.The mechanisms,by which n-butanol azeotropic distillation prevents the formation of hard agglomerates,were attributed both to the decrease of capillary force during drying process between the particles,because of the substitution of n-butanol for water,and to the physical absorption of OC4H9 on the surface of the hydrates particles,thereby completely breaking down the hydrogen bonds between the particles." @default.
- W2366127194 created "2016-06-24" @default.
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- W2366127194 date "1996-01-01" @default.
- W2366127194 modified "2023-09-25" @default.
- W2366127194 title "Preparation and Mechanism of Nanometer Sized Agglomeration-free Al_2O_3-ZrO_2 Powders" @default.
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