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- W2366698907 abstract "OBJECTIVE To study the preparation of sultamicillin tosilate gelatin microspheres granules and its quality control.METHODS Sultamicillin tosilate gelatin microspheres granules were prepared by mixing sultamicillin tosilate gelatin microspheres with appropriate excipients.The sample was extracted with(0.1 mol)·L~(-1) hydrochloride solution by ultrasonication.RP-HPLC was used for the determination of sultamicillin tosilate in sultamicillin tosilate gelatin microspheres granules.The chromatographic procedure was carried out using Dionex Kromasil ODS1((250 mm)×(4.6 mm),(5 μm)) as an analytical column and a mixture of 85 volume of(0.02 mol)·L~(-1) sodium dihydrogen phosphate solution and 15 volume of acetonitrile(the pH was adjusted to(4.4) with phosphoric acid) as mobile phase.The detection wavelength was(218 nm).RESULTS The granules was a almost white powder and sweet.Other tests conformed to the requirements.The retention time of Sultamicillin Tosilate was about 6 minutes and the resolution was more than(1.5).Tt's linear ranges were between(0.128)~(0.642 mg)·mL~(-1).The average recoveries(n=3) of high,middle,low three concentrations were(101.3%),(100.8%),(100.3%);RSDs were(0.18%),(0.35%),(0.33%).CONCLUSION This preparation can completly remove the bitter taste of sultamicillin tosilate,and is suitable for children.The quantitati on method is simple、accurate、reliable,and can be used as the quality control of this preparation." @default.
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- W2366698907 date "2005-01-01" @default.
- W2366698907 modified "2023-09-23" @default.
- W2366698907 title "Study on the preparation of sultamicillin tosilate gelatin microspheres granules and its quality control" @default.
- W2366698907 hasPublicationYear "2005" @default.
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