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- W2366932783 abstract "By testing all related factors which have effects on microwave digestion,optimizing the operation conditions of graphite furnace atomic absorption spectrometry(GFAAS),the research establishes a sensitive,effective method to determine lead(Pb),cadmium(Cd) in animal bones.The result has shown that the optimized condition for microwave digestion is: digestion pressure 15 MPa,digestion length 5 min.The best condition for graphite furnace is: Pb(lead) ashing temperature 800 ℃,atomization temperature 1 300 ℃;Cd(cadmium) ashing temperature 900 ℃,atomization temperature 1 200 ℃.The methodical linearity range is Pb 1.566~50 ng/mL;Cd 0.0745~5 ng/mL.The methodical detection limit is Pb 0.3132 ng/mL;Cd 0.0149 ng/mL.The tested RSD of the sample is less than 5%,and the sample assaying recovery rate is between 88.36% and 110%." @default.
- W2366932783 created "2016-06-24" @default.
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- W2366932783 date "2007-01-01" @default.
- W2366932783 modified "2023-09-24" @default.
- W2366932783 title "Microwave digestion of animal bones and determination of lead and cadmium by graphite furnace atomic absorption spectrometry" @default.
- W2366932783 hasPublicationYear "2007" @default.
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