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- W2366946006 abstract "A TiO2 nanotubes(TNTs) array was obtained on pure titanium substrate by anodic oxidation in 1.0wt% HF solution. The surface morphology and phase structure of the TNTs array were characterized by scanning electron microscopy and X-ray diffraction. The heat treatment at 450 °C changes the TNTs from amorphous structure to anatase form. A Ti3+-doped TNTs was prepared by electrochemical reduction of the heat-treated TNTs array in 1.5 mol/L(NH4)2SO4 electrolyte. The influence of self-doping time on conductivity of the TNTs was studied by electrochemical impedance spectroscopy. The results of X-ray photoelectron spectroscopy showed that nearly 42.9% Ti4+ in TNTs was reduced to Ti3+ after electrochemical self-doping at-1.45 V(vs. saturated calomel electrode) for 60 s, thus efficiently decreasing the impedance of TNTs after the formation of anatase phase." @default.
- W2366946006 created "2016-06-24" @default.
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- W2366946006 date "2014-01-01" @default.
- W2366946006 modified "2023-09-23" @default.
- W2366946006 title "Preparation of Ti~(3+)-doped TiO_2 nanotube array and its electrochemical impedance spectroscopic study" @default.
- W2366946006 hasPublicationYear "2014" @default.
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