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- W2366949462 abstract "A method was established for simultaneous determination of 15 phthalic acid esters(PAEs) in alcohol by ultra performance liquid chromatography-tandem mass spectrometry(UPLC-MS / MS).Liquid-liquid extraction(LLE) approaches have been used for isolation of PAEs from alcohol samples,which were salted out by sodium chloride at the same time.After that,the extract solution was dried within nitrogen.In the chromatographic analysis,15 target compounds were separated on an Agilent SB C18 column with gradient elution using mobile phase of acetonitrile and water containing 15 mmol / L ammonium acetate.Multiple reaction monitoring(MRM) acquisition under positive ion mode was performed.As a result,the detection limits(CCα) of the target compounds were from 0.8μg / L to 3.4μg / L in alcohol and the quantitation limits(CCβ) were from 1.2μg / L to 5.1μg / L.The intra-day precision of the 15 analytes spiked at three concentration levels ranged from 82.6% to 109.2% with the relative standard deviations(RSD) of 2.2% ~ 14%,while the inter-day precisions ranged from 82.0% to 109.6% with the RSD of 2.6% ~ 12%.The method can be applied to the analysis of PAEs in alcohol." @default.
- W2366949462 created "2016-06-24" @default.
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- W2366949462 date "2013-01-01" @default.
- W2366949462 modified "2023-09-23" @default.
- W2366949462 title "Determination of 15 phthalates in alcohol by ultra performance liquid chromatography-tandem mass spectrometry" @default.
- W2366949462 hasPublicationYear "2013" @default.
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