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- W2367285868 abstract "A fast and precise method for the determination of acrylamide in fried instant noodles with high performance liquid chromatography (HPLC) was established.The method is based on extraction of acrylamide with 1 g/L HCOOH solution.The aqueous sample solution was centrifuged twice at 12,000 rpm,2 ℃ and 14,500 rpm,0 ℃ for 18 min to successfully remove the amylum,protein and fat in the samples.The method was optimized for the determination of acrylamide in fried instant noodle samples as follows:separation is carried out on a column of ZORBAX SB-C18 (250×4.6 mm i.d 5 μm) with A (acetonitrile and ultra-high purity water 1:24,V/V) and B (acetonitrile) as the mobile phase,at elution flow rate of 0.5 mL/min and maximum absorption UV wavelength of 197 nm for detecting acrylamide.The experimental results show a good linear relationship between the peak area and the concentration (r=1.00000).Detection limit of the method is 48.0 μg /kg.The recoveries ranged from 94.4% to 109.8% with relative standard deviations between 4.7% and 5.6%.This method was simple,precise and had high recoveries,which could be used for the determination of acrylamide in fried instant noodle samples." @default.
- W2367285868 created "2016-06-24" @default.
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- W2367285868 date "2010-01-01" @default.
- W2367285868 modified "2023-09-25" @default.
- W2367285868 title "The determination of acrylamide in fried instant noodles with high performance liquid chromatographic method" @default.
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