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- W2367716217 abstract "The preparation process of trimesic from mesitylene by air in a liquid phase oxidation under normal pressure with the catalysis of cobalt acetate and sodium bromide was studied.The product was confirmed as trimesic by using acid value titration,IR spectrum and liquid chromatogram.By studying the effects of reaction conditions,such as types of reactors,reaction temperature,reaction time and catalyst,the optimum conditions were given as followings:n(mesitylene)∶n(acetic acid)∶n(cobalt acetate)∶n(sodium bromide)∶n(sodium acetate)=1∶35∶0.2∶0.1∶0.05; concentration of Co2+ was 0.094 mol/L; the reaction takes place in a bubbling reactor at 95℃ for 4.5 h.Under these conditions the trimesic yield can reach 43.56%,with 752.39 mg/g of trimesic's acid value and 96.46% of purity." @default.
- W2367716217 created "2016-06-24" @default.
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- W2367716217 date "2003-01-01" @default.
- W2367716217 modified "2023-09-24" @default.
- W2367716217 title "Synthesis of trimesic from liquid phase oxidation of mesitylene by air" @default.
- W2367716217 hasPublicationYear "2003" @default.
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