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- W2367843668 abstract "The O,Odialkylphosphorochloridothionates(A) were synthesized by the reaction of thiophosphoryl chloride with long chain alcohol and phase transfer catalysis (PTC) in the presence of alkali. Long chain bis-(thiophosphoryl) imines were obtained from aminolysis of A and condensation between A and (RO)2PSNH2. The optimum reaction conditions were obtained: BuNBr was used as PTC for preparing O,O-dialkylphosphorochloridothion-ates,its quantity was 3% mole of long chain alcohol ; the ratio of PSC13:alcohol : NaOH was 1 = 2:2.5; reaction time;4 hours; reaction temperature: 40℃. NaH was the best base in the preparation of bis-(thiophosphoryl) imines . The compounds were characterized by elemental analysis,IR and HNMR." @default.
- W2367843668 created "2016-06-24" @default.
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- W2367843668 date "2003-01-01" @default.
- W2367843668 modified "2023-09-27" @default.
- W2367843668 title "Synthesis of long chain bis-( thiophosphoryl) imines by phase transfer catalysis" @default.
- W2367843668 hasPublicationYear "2003" @default.
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