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- W2367846952 abstract "Under the following reaction conditions- temperature 50 - 70C℃ , pressure 1.0 - 2.0 MPa, solvent C6D6, initiator AIBN, the reactions of 1, 5 - cyclooctadiene, dicyclopentadiene, 1,3-cyclohexadiene, 1,4 - cyclohexadiene and 1,5,9 - cyclododecatriene with PH3 were studied by using the pressurized in - situ NMR technique. Experimental results indicated that the bicyclophosphanonane was formed by the addition of PH3 to 1,5 - cyclooctadiene. On the other hand, the heterocyclic compounds containing phosphorus could not be obtained in the-reactions of PH3 with other three cyclic olefins, primary phosphines being the only products observed. The results also indicated that the reactions of PH3 with cyclic olefins proceeded with a sequential mechanism." @default.
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- W2367846952 date "1996-01-01" @default.
- W2367846952 modified "2023-09-24" @default.
- W2367846952 title "In situ (31)~P NMR Study on the Reaction of Cyclic Olefins with Phosphine" @default.
- W2367846952 hasPublicationYear "1996" @default.
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