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- W2368005320 abstract "A new system of cambridge filter trapping device-thermogravimetry-gas chromatography-mass spectrometry wasestablished and applied to study the formation of benzo(a) pyrene in low temperature cellulose pyrolysis by collectingsamples in different temperature ranges.Cambridge filter trapping device was used to collect evolved gas in 270℃-450℃ and 450℃-600℃ under flowing nitrogen of 200 mL/min and heating rate of 10 ℃ /min.Benzo [a] pyrene was qualita-tively and quantitatively analyzed by gas chromatography/mass spectrometry(GC/MS) after extracting from the trappedcambridge filter.Results showed that 1) applying small cambridge filter(8 mm in diameter) and keeping same flow rate of carrier gas at both entrance and exit of cambridge filter was the optimal condition based on trapping effect of benzo [a] pyrene;2) benzo[a]pyrene yield in 450℃-600℃ temperature range was higher than that of 270℃-450℃;and 3) reli-ability of this system was verified since yields of benzo [a] pyrene was very close to quoted value and RSDs(n=3) wereall below 10%." @default.
- W2368005320 created "2016-06-24" @default.
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- W2368005320 date "2012-01-01" @default.
- W2368005320 modified "2023-09-23" @default.
- W2368005320 title "The formation of benzo [a] pyrene in low temperature cellulose pyrolysis with cambridge filter trapping device-thermogravimetry-gas chromatography mass spectrometry" @default.
- W2368005320 hasPublicationYear "2012" @default.
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