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- W2368127679 abstract "For pretreatment, the Siraitia grosvenorii samples were pre-dissolved by nitric acid and hydrogen peroxid with the XT-9800 multifunctional heating device, then were digested completely using XT-9900 intelligent microwave digestion device.The three procedures of microwave digestion were:0.3MPa/120s,0.5MPa/240s,1.0MPa/90s.The compromise measurement conditions of inductively coupled plasma using axial viewing mode were RF power 1100W, carrier gas current 0.8L·min-1. The results of two kinds of Siraitia grosvenorii samples were satisfying. RSD(%,n=5)Al 1.21~9.81, Cd 0.89~1.18,Cu 0.85~4.72,Fe 4.48~6.71, Mg 0.27~1.16, Mn 0.51~1.00,P 0.20~0.91,Pb 0.86~4.33, Zn 0.042~0.87, recovery(%)Al 102.0~105.0, Cd 97.0~102.0, Cu 104.0, Fe 96.4~97.8, Mg 96.0~97.0, Mn 96.0~100.0, P 92.0~99.0, Pb 93.09~6.0, Zn 91.01~05.0." @default.
- W2368127679 created "2016-06-24" @default.
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- W2368127679 date "2008-01-01" @default.
- W2368127679 modified "2023-09-28" @default.
- W2368127679 title "High Pressure Microwave Digestion and Determination of Microelements Siraitia grosvenorii by ICP-AES" @default.
- W2368127679 hasPublicationYear "2008" @default.
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