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- W2368132371 abstract "OBJECTIVE To study the influence of salt,ester,proteins in biological specimens on determination of clozapine concentration by Solid-phase microextraction-Gas Chromatography Mass Spectrometry(SPME-GC-MS).METHODS Clozapine and loxapine(internal standard)in these samples were detected by SPME-GC-MS,and the influence of solt,ester,proteins were observed by content variety of NaCl,ethyl acetate and plasma.RESULTS With the increased of content of salt in sample,peak areas of clozapine and loxapine increased and method sensitivity raised.With the increased of content of ester or proteins in sample,peak areas of clozapine and loxapine decreased and method sensitivity lowered.The peak areas of clozapine and loxapine had the same change tendency and peak area ratios of them remained almost constant in each group.CONCLUSION The changes of contents of salt,ester,proteins in samples will influence sensitivity of detection of clozapine by SPME-GC-MS,but the accuracy of quantitative analysis will not be influenced if suitable internal standard used." @default.
- W2368132371 created "2016-06-24" @default.
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- W2368132371 date "2007-01-01" @default.
- W2368132371 modified "2023-09-27" @default.
- W2368132371 title "The influence of biological specimen ingredient on determination of clozapine concentration in biological specimens" @default.
- W2368132371 hasPublicationYear "2007" @default.
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