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- W2368586721 abstract "Nano-sized ZnO particles were prepared by using zinc sulfate and sodium hydroxide as raw materials in the membrane dispersion micro-structured reactor by rapid mixing precipitation.The mixing scale model was used to simulate the precipitation process of nucleation,growth and agglomeration in the membrane reactor.Modeling results showed that particle nucleation dominated in the initial 0.6ms,and after 1.6ms,growth dominated.At the same time,due to a large number of particles,particles collision would cause aggregation,resulting in specific distribution of particle size.Mixing scale and reactant concentration had a great influence on particle diameter and distribution.Simulation results showed that when mixing scale reduced from 50μm to 5μm,average diameter of nano-ZnO particles decreased to 12nm from 19nm.Experimental results showed that with the decrease of membrane pore size,average diameter of nano-ZnO particles dropped down from 20 nm to 11 nm,and when initial reactant concentration increased from 0.05mol·L-1 to 0.20mol·L-1,average diameter of ZnO nanoparticles increased from 10nm to 16nm.Simulated average particle diameter and its distribution agreed well with the experimental values." @default.
- W2368586721 created "2016-06-24" @default.
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- W2368586721 date "2013-01-01" @default.
- W2368586721 modified "2023-09-24" @default.
- W2368586721 title "Preparation of nano-ZnO in membrane dispersion micro-reactor and modeling" @default.
- W2368586721 hasPublicationYear "2013" @default.
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