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- W2368640211 abstract "NaInS2 microspheres were successfully synthesized by a new one-step solvothermal method via selfdecomposition of In(S2CNEt2)3complex under the condition of excess NaEt2CNS2 at 200 ℃,with acetonitrile and oleic acid(OA)as solvent and surfactant,respectively.A special nanosheet acanthosphere can be easily obtained by adjusting the OA content of reaction solvent.According to the XRD and FE-SEM results,the achieved NaInS2 was well-crystallized with rhombohedral structure and single phase.The addition of OA had significant effects on the micro-structure of the obtained NaInS2 microspheres.When a little OA(5mL)were added,it had no obvious effect on the composition and crystallinity of NaInS2 microspheres.But it would change the structure of the products from solid microspheres into porous ones comprised by primary particles.When OA content was more than 10 mL,clear preferred orientation growth would take place on the primary particles of the microsphere,which finally made the microspheres turned into nanosheet acanthospheres with large porosity.In addition,the diffuse reflectance spectra suggested that the prepared NaInS2 microspheres presented strong absorption to the light whose wavelength was less than 450nm(absorption boundary at 450nm).However,the absorption boundary of the nanosheet acanthospere was 400 nm with 50 nm blue shift.PL spectra manifested that a broad emission band(340-650nm)peaked at 394 nm can be observed under 245 nm UV excitation,which was due to the inter-band electronic transition of NaInS2." @default.
- W2368640211 created "2016-06-24" @default.
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- W2368640211 date "2015-01-01" @default.
- W2368640211 modified "2023-09-25" @default.
- W2368640211 title "Synthesis of NaInS_2 nanosheet acanthosphere by one-step solvothermal decomposition of single-source molecular complex" @default.
- W2368640211 hasPublicationYear "2015" @default.
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