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- W2368851097 abstract "With the acrylonitrile and the diacetone alcohol as raw materials,the orthogonal test and proving test aim to get the best process condition of the synthesis of 5,6-dihydro-4,4,6-trimethyl-2-vinyl-6-hydroxy-1,3-(4H)-oxazine sulfate(1:1).The feeding temperature is 10～15 ℃;the ratio of the amount of diacetone alcohol, acrylonitrile and oil of vitriol is 1.2:1.0:2.2～2.5;the time for reaction in a constant temperature is about 3 hours;and the stirring time after adding acetone is 1 hour." @default.
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- W2368851097 date "2007-01-01" @default.
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- W2368851097 title "Research on the synthesis of oxazine sulfate" @default.
- W2368851097 hasPublicationYear "2007" @default.
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