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- W2369047402 abstract "HPLC was applied to monitor the esterification reaction,which is an important reaction in the synthesis of ethyl-L-thiazolidine-4-carboxylate.Chromatography conditions:YMC-Pack Pro C18 RP column(4.6 mm×150 mm×5 μm);mobile phase:0.01 mol/L monosodium phosphate-methanol(97∶3);detection wavelength:210 nm;flow rate:1.0 mL/min.The calibration curve was linear in the range of 0.158~1.278 mg/mL of esterification reaction mixture with r=0.997 6.The average recovery was 94.70% while the relative standard deviation for repetitions was 0.08%~1.62%.This method has the advantages of quick,correct,reapprearing." @default.
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- W2369047402 date "2013-01-01" @default.
- W2369047402 modified "2023-09-26" @default.
- W2369047402 title "Esterification reaction of ethyl-1-thiazolidine-4-carboxylate monitored by HPLC" @default.
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