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- W2369685352 abstract "Objective:To establish a capillary zone electrophoresis method for the chiral separation and determination of R-isomer of tirofiban hydrochloride.Methods:A chiral separation was completed by optimizing separation factors including types and concentrations of cyclodextrin,the pH value and concentration of the buffer used,and the voltage and temperature during the separation.Results:The separation was performed with a 46-cm length of 75 μm i.d.fused-silica capillary.Well-defined separation of R-isomer and tirofiban hydrochloride(S) was achieved in the 50 mmol·L-1 phosphate buffer(pH 2.0,with 0.6 mmol·L-1HP-γ-CD)-methanol(95∶ 5) running buffer,and detected at 200 nm,18 kV of the applied voltage and 15 ℃ of separation temperature.Conclusion:The method developed in this study is simple and fast.It can be used for the quality control of R-isomer of tirofiban hydrochloride." @default.
- W2369685352 created "2016-06-24" @default.
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- W2369685352 date "2014-01-01" @default.
- W2369685352 modified "2023-09-25" @default.
- W2369685352 title "Chiral separation of tirofiban hydrochloride by capillary zone electrophoresis" @default.
- W2369685352 hasPublicationYear "2014" @default.
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