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- W2369863669 abstract "Nanocrystalline silver sulfide was successfully synthesized at room temperature and ambient pressure via a novel, safe, convenient and inexpensive redox reaction, using silver oxide, sulfur and polyformaldehyde as reactants and ethylenediamine as solvent. The products were characterized with XPS, XRD and TEM. XRD spectrum demonstrates a monoclinic Ag 2S; TEM shows the products are rod-like nanoparticles with average diameter of 100 nm, its corresponding SAED reveals clear diffraction spots indexed as (120) and (3-03); XPS confirms the formation of Ag 2S and indicates the sample's surface stoichiometry of Ag∶S=1∶0.453. The control experiments show polyformaldehyde and ethylenediamine are both important in the formation of products. Ethylenediamine accelerates the reactions via dissolving silver oxide and sulfur and neutralizing the by-product formic acid." @default.
- W2369863669 created "2016-06-24" @default.
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- W2369863669 date "2005-01-01" @default.
- W2369863669 modified "2023-09-24" @default.
- W2369863669 title "Synthesis of Ag_2S Nanoparticles at Room Temperature and TheirCharacterization with XPS" @default.
- W2369863669 hasPublicationYear "2005" @default.
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