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- W2369893758 abstract "The title compound,[n-Bu_(4)N]~(+)[FeCl_(4)]~(-) was prepared and characterized by elemental analysis and X-ray crystallography.It crystallizes in the orthorhombic system,space group Pnna,a=1.851 0(4) nm,b=1.155 3(2) nm,c=1.144 2(2) nm,V=2.446 8(8) nm~(3),Z=8,D_(c)=1.195 g·cm~(-3),F(000)=932,μ =1.051 mm~(-1).The crystal structure consists of one independent [FeCl_(4)]~(-)anion and one independent([n-(Bu_(4)N)]~(+))cation.In [FeCl_(4)]~(-)anion,the central Fe atom adopts distorted tetrahedral geometry with four Cl atoms,and Fe-Cl bond distances are 0.212 2(14) nm and(0.218 07)(17) nm respectively.In [n-Bu_(4)N]~(+) cation,N atom also adopts a slightly distorted tetrahedral geometry.In the solid state,the C-H…Cl interactions link [FeCl_(4)]~(-) anions and [n-Bu_(4)N]~(+) cations which stabilize the structure." @default.
- W2369893758 created "2016-06-24" @default.
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- W2369893758 date "2006-01-01" @default.
- W2369893758 modified "2023-09-28" @default.
- W2369893758 title "Synthesis and Crystal Structure of Tetrabutylammonium Tetrachloroferrate Complex" @default.
- W2369893758 hasPublicationYear "2006" @default.
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