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- W2369931289 abstract "Liquid chromatography-tandem mass spectrometry( LC-MS /MS) was used for the simultaneous quantitative analysis of nonylphenol( NP),octylphenol( OP),bisphenol A( BPA),4-tert-butylphenol( POP),2,4-dichorophenol( 2,4-DCP) and 4-tert-octylphenol( PTBP) in some marine organisms. Samples were extracted and purified by accelerated solvent extraction( ASE) and a NH 2 solid extraction cartridge. LC was equiped with a Waters Symmetry-C18 column,and the mobile phase methanol and 2% ammonia solution was chosen and gradient elution. MS / MS was operated in the negative electron spray ionization utilizing multiple reaction monitoring mode. The recoveries of target compounds were 67. 0% ~ 89. 0% with the relative standard deviations ranged from 4. 3% to 8. 5%. The detection limits of method were 1. 0 × 10- 9to 1. 2 × 10- 9. Five kinds of biological samples were analyzed and the results showed that six phenolic endocrine disruptors existed in all sorts of organisms with the concentrations ranging from undetected to384 × 10- 9. The method validation and actual sample analysis indicated that this method was sensitive,accurate and precise,so it was adapt to analyze the phenol compounds in the organisms." @default.
- W2369931289 created "2016-06-24" @default.
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- W2369931289 date "2014-01-01" @default.
- W2369931289 modified "2023-09-25" @default.
- W2369931289 title "Development and application of a method to determine phenolic endocrine disruptors in marine organisms" @default.
- W2369931289 hasPublicationYear "2014" @default.
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