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- W2369980557 abstract "The catalytic activity of KF/MgO for the synthesis of didodecyl carbonate(DDC) by transesterification of dimethyl carbonate(DMC) with dodecanol(DoOH) was studied.The effects of KF loading and calcination temperature were investigated.The catalysts were characterized by X-ray diffraction,Fourier transform infrared spectroscopy,scanning electron microscopy,and N2 adsorption-desorption.The results indicated that new phases K2MgF4 and K2CO3 were formed when KF/MgO was calcined in air at high temperature.K2MgF4 and K2CO3 were the main catalytic sites in this reaction.KF/MgO was an effective catalyst in this transesterification reaction and the optimized KF loading and calcination temperature were 30% and 873 K,respectively.The optimized reaction conditions were as follows:n(DoOH):n(DMC)=4,catalyst amount 0.75%,reaction time 4 h.Under these conditions,the conversion of DMC and the yield of DDC were 86.7% and 86.2%,respectively." @default.
- W2369980557 created "2016-06-24" @default.
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- W2369980557 date "2010-01-01" @default.
- W2369980557 modified "2023-09-26" @default.
- W2369980557 title "Transesterification of Dimethyl Carbonate with Dodecanol to Didodecyl Carbonate over KF/MgO Catalyst" @default.
- W2369980557 hasPublicationYear "2010" @default.
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