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- W2370116758 abstract "After expounding Musk xylene's nature,application and influence on the life and environment,the synthesis of musk xylene was carried out by three-step method in order to monitor the production process of suppliers.At first,tert-butyl chloride—the alkylation's agent,was synthesized by hydrochloride acid reacting with tert-butyl alcohol.Relatively high yield 89.58% was got by controlling the reaction temperature higher than tert-butyl chloride's boiling point,and then the product—tert-butane chlorinated was being distillated out of the reactor directly when the reaction happened.At the second step,tert-butyl-m-xylene was synthesized by reacting chlorinate tert-butane with m-xylene in the presence catalyst of anhydrous aluminum chloride.Based on orthogonal test,the suitable conditions were established.The optimum reaction conditions were as follows:Molecule ratio of m-xylene/chlorinated tert-butane/ anhydrous aluminum chloride molar 8∶1∶0.04,reaction temperature 0℃,reaction time 4h,and the yield of product was about 86.97%.The total yield of musk xylene is about 65.00% based on the amount of m-xylene.The chemical structure of the main products are characterized by IR and melt point." @default.
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- W2370116758 date "2009-01-01" @default.
- W2370116758 modified "2023-09-24" @default.
- W2370116758 title "Environmental & Ecological Effect of Musk Xylene and Its Synthesis" @default.
- W2370116758 hasPublicationYear "2009" @default.
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