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- W2370152772 abstract "Objective:To establish a rapid,simple,which can be used for batch samples new method for determination of Urinary iodine.Methods: According to the reaction principle for ammonium persulfate digestion As-Ce catalytic spectrophotometry,60 micro urine samples were simultaneously sealed and digested in a 96-well microplate,then the absorbance of the samples were simultaneously measured by the ELIASA,so the contents of iodine in 60 urine samples were obtained at the same time.Results: The losses and cross contamination of samples weren′t found in the 96-well microplate when digestion and determination.The method was liner in the range of 0 μg/L~300 μg/L,the regression equation:C(μg/L)=17.68-367.4lgA,R=0.9985,the within and between RSDs were 2.32%~5.60% and 4.50%,respectively the rates of recovery were 93.3%~105.9%.The determination results of iodine in 60 urine samples by the method were agreed with those obtained by the standard method.Conclusion: The method is less regents consumption,simple,rapid,accurate and reliable,it is suitable for analysis of large number of samples.Based on the above,this method has high value in practical application." @default.
- W2370152772 created "2016-06-24" @default.
- W2370152772 creator A5003317924 @default.
- W2370152772 date "2011-01-01" @default.
- W2370152772 modified "2023-09-24" @default.
- W2370152772 title "Study on the determination of urinary iodine in 96-well microplate" @default.
- W2370152772 hasPublicationYear "2011" @default.
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