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- W2370298214 abstract "In order to find out optimal conditions for the column chromatographic isolation of 5-chloroanthranilic acid from urine, three columns were tested. The best isolation is obtained by ion-exchange chromatography on a column packed with Zerolite 225 (200～300 mesh), the column is eluted at 25～30 ml/hr with 80 ml 0.5M Na_2HPO_4 solution. Recovery of 5-chloroanthnanilic acid from urine is 76～90%. The sample obtained from the procedure can be chromatographed on Silica Gel H/benzen-dioxaneacetic acid (95: 25: 4) and 5-chloroanthranilic acid is defected by spraying with 1% NaNO_2 in 1N HCI followed by spraying with 0.4% N- (1-naphthyl)-ethylenediamine, and 0.1μg of the compound can be detected. The identification of the compound in urine has been confirmed by fluorescence spectrum." @default.
- W2370298214 created "2016-06-24" @default.
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- W2370298214 date "1981-01-01" @default.
- W2370298214 modified "2023-09-22" @default.
- W2370298214 title "STUDIES ON ANALYSIS OF METABOLITES OF PESTICIDES II. ISOLATION AND TLC OF 5-CHLOROANTHRANILIG ACID IN URINE" @default.
- W2370298214 hasPublicationYear "1981" @default.
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