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- W2370320714 abstract "Objective To establish a method for simultaneous determination of naringin,hesperidin and neohesperidin in dysmenorrhea patches by HPLC. Methods The HPLC method was validated using a Cosmosil C18 analytical column( 5 μm,4. 6 mm × 250 mm) and the mobile phase was acetonitrile- 0. 1% phosphoric acid( 21∶ 79) at a flow rate of 1. 0 m L·min~(-1)with UV detection at 283 nm. The column temperature was kept at 25℃ and the injection volume was 10 μL. Results The linear ranges of naringin,hesperidin and neohesperidin were 10. 63 ~ 340 mg·L~(-1),7. 81 ~ 250 mg·L~(-1)and 8. 13 ~ 260 mg·L~(-1),respectively. The average sample recovery rates were 98. 01 %,97. 90 % and 98. 60 %,respectively. Conclusion The method is simple,accurate and reliable,which can be used for quality control of dysmenorrhea patches." @default.
- W2370320714 created "2016-06-24" @default.
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- W2370320714 date "2015-01-01" @default.
- W2370320714 modified "2023-09-25" @default.
- W2370320714 title "Simultaneous determination of naringin,hesperidin and neohesperidin in dysmenorrhea patches by HPLC" @default.
- W2370320714 hasPublicationYear "2015" @default.
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