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- W2371034080 abstract "OBJECTIVE:To establish a HPLC method for the simultaneous determination of aspirin and phenobarbital in aspirin and phenobarbital sugar pills.METHODS:Aspirin and phenobarbital were seperated on Inertsil C8-3 column with column temperature at 40℃.The mobile phase consisted of methanol-0.05mol·L-1NaH2PO4 buffer solution(50∶50)with flow rate at 1.0mL·min-1.The detection wavelength was set at 210 nm and the sample size was 20μL.RESULTS:The linear ranges for aspirin and phenobarbital were 31.15～498.40(r=0.999 9)and 3.2～51.2μg·ml-1(r=0.999 9),respectively.The average recoveries were 101.18%(RSD=1.9%)and 100.73%(RSD=1.7%),respectively.CONCLUSION:This method is simple,rapid,and accurate and reliable,and it can be used as a quality control of aspirin and phenobarbital sugar pills." @default.
- W2371034080 created "2016-06-24" @default.
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- W2371034080 date "2007-01-01" @default.
- W2371034080 modified "2023-09-26" @default.
- W2371034080 title "Determination of Aspirin and Phenobarbital in Aspirin and Phenobarbital Sugar Pills by HPLC" @default.
- W2371034080 hasPublicationYear "2007" @default.
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