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- W2371126952 abstract "3-Amino-triazole-5-carboxylic acid was proposed by acylating and cyclizating in condition of aminoguanidine and oxalic acid.Factors were investigated including the material ratio,mother liquor,reaction temperature and water consumption.The yield and purity of 3-Amino-triazole-5-carboxylic acid were 76.8% and 95.67% respectively under the optimal conditions:n(oxalicacid)n(aminoguanidine)=1.31,mother liquor was applied twice,sulfuric acid was completed dropping 1 h at 60 ℃ and m(acylation)m(water consumption)=15.The synthetic compounds were characterized by IR,1H NMR and mass spectra." @default.
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- W2371126952 date "2011-01-01" @default.
- W2371126952 modified "2023-09-24" @default.
- W2371126952 title "Synthesis technology of 3-Amino-triazole-5-carboxylic acid" @default.
- W2371126952 hasPublicationYear "2011" @default.
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