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- W2371505012 abstract "Sintered Nb2O5 powder compacts,used as the cathode,were electrodeoxidized in eutectic melt of CaCl2-NaCl.The influence of sintering temperature on porosity of cathodes,deoxidization and the products resulted was studied.Sintered Nb2O5 powder compacts and electrolysis products were analyzed by XRD,SEM,EDS.The results showed that sintering temperature had great influence on grain size and porosity of sintered Nb2O5 powder compacts.Open porosity benefits permeability of melt and expansion of reaction interface which accelerates the rate of deoxidization.The rate of deoxidization depends on not only open porosity but also porosity size.The results showed that oxygen content of the cathode sintered at 1 200 ℃ for 12 h can be lowest." @default.
- W2371505012 created "2016-06-24" @default.
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- W2371505012 date "2011-01-01" @default.
- W2371505012 modified "2023-09-24" @default.
- W2371505012 title "Influence of Sintering Temperature on Preparation of Niobium by Direct Electrochemical Reduction of Solid Nb_2O_5" @default.
- W2371505012 hasPublicationYear "2011" @default.
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