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- W2371566483 abstract "Using 5-(2-(1H-imidazol-1-yl)-2-oxoethyl)benzo[b]acridin-12(5H)-one(IEBA)as a new pre-column derivatization reagent,six aromatic amine compounds could be baseline separated on a reversed-phase Akasil-C18 column in conjunction with a gradient elution in 25 min.Detection was also carried out by online post-column atmospheric pressure chemical ionization(APCI)in the positive-ion mode.The nucleophilic substitution product of IEBA and aromatic amines not only have high fluorescence sensitivity but also have strong ionizable ability.Based on these facts,a rapid,accurate method for the determination of aromatic amines in hair dye was proposed.The established method exhibited excellent reproducibility and recovery.Excellent linear responses were observed with the correlation coefficients 0.9999.The detection limits(at signal-to-noise of 3∶1)were 0.19～0.04 ng/mL." @default.
- W2371566483 created "2016-06-24" @default.
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- W2371566483 date "2010-01-01" @default.
- W2371566483 modified "2023-09-23" @default.
- W2371566483 title "Aromatic Amines Using 5-(2-(1H-imidazol-1-yl)-2-oxoethyl)benzo[b]acridin-12(5H)-one as Novel Fluorescence Labeling Reagent and Their Mass Spectrometric Identification" @default.
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